Film washing problem?

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I seem to be having a problem with film washing as evident by the line of crap running horizontally across the image through Barbie's left eye shown here http://users.imag.net/~lon2251/temp/barbie.jpg. 

I washed the film with tap water. Then with the film still in the developing tank, I filled the tank with distilled water and two drops of LFN that I purchased a week ago. I agitated it in there for about twenty seconds then hung the film and squeegeed it with my wet fingers.  Obviously I've done something wrong. Can anyone help me clear this up?

Thanks, Greg


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